Use of interelectrode material transfer of nickel and copper‑nickel alloy to carbon fibers to assemble miniature glucose sensors

Rozsypal, Jan; Říman, Daniel; Halouzka, Vladimír; Opletal, Tomáš; Jirovský, David; Prodromidis, Mamas; Hrbáč, Jan

dc.title	Use of interelectrode material transfer of nickel and copper‑nickel alloy to carbon fibers to assemble miniature glucose sensors	en
dc.contributor.author	Rozsypal, Jan
dc.contributor.author	Říman, Daniel
dc.contributor.author	Halouzka, Vladimír
dc.contributor.author	Opletal, Tomáš
dc.contributor.author	Jirovský, David
dc.contributor.author	Prodromidis, Mamas
dc.contributor.author	Hrbáč, Jan
dc.relation.ispartof	Journal of Electroanalytical Chemistry
dc.identifier.issn	1572-6657 Scopus Sources, Sherpa/RoMEO, JCR
dc.date.issued	2018
utb.relation.volume	816
dc.citation.spage	45
dc.citation.epage	53
dc.type	article
dc.language.iso	en
dc.publisher	Elsevier
dc.identifier.doi	10.1016/j.jelechem.2018.03.039
dc.relation.uri	https://www.sciencedirect.com/science/article/pii/S1572665718302091
dc.subject	Non enzymatic glucose sensor	en
dc.subject	Anodic dissolution	en
dc.subject	Nickel nanoparticles	en
dc.subject	Copper nickel alloyed nanoparticles	en
dc.subject	Carbon fiber microelectrode	en
dc.description.abstract	Electrochemical deposition of the material released by anodizing nickel and copper nickel alloy in pure water onto carbon fiber microelectrodes was used to assemble miniature glucose sensors. The composition and morphology of the deposits was investigated by scanning electron microscopy, energy dispersive X-ray spectroscopy and X-ray photoelectron spectroscopy. The deposition of anode-derived materials proceeded by two consecutive mechanisms, which are explained in detail. The electrochemical properties of the designed electrodes were subsequently investigated by cyclic voltammetry and electrochemical impedance spectroscopy. The different Ni- and mixed CuNi-modified microelectrodes were examined as glucose sensors and the best performing electrodes based on the alloyed deposit exhibited very high sensitivity (5720 μA mM−1 cm−2), low detection limit (0.3 μM) and ability to quantify glucose in blood serum. © 2018 Elsevier B.V.	en
utb.faculty	Faculty of Technology
dc.identifier.uri	http://hdl.handle.net/10563/1007815
utb.identifier.obdid	43878916
utb.identifier.scopus	2-s2.0-85044141483
utb.identifier.wok	000431156900007
utb.identifier.coden	JECHE
utb.source	j-scopus
dc.date.accessioned	2018-04-23T15:01:46Z
dc.date.available	2018-04-23T15:01:46Z
dc.description.sponsorship	15-05198S, GACR, Grantová Agentura České Republiky
dc.description.sponsorship	Grant Agency of the Czech Republic [15-05198S]; Palacky University [IGA_PrF2018_027]
utb.contributor.internalauthor	Halouzka, Vladimír
utb.fulltext.affiliation	Jan Rozsypal a , Daniel Riman a , Vladimir Halouzka b,c , Tomas Opletal a , David Jirovsky a , Mamas Prodromidis d , Jan Hrbac e,⁎ a Department of Analytical Chemistry, Palacky University, Faculty of Science, 17. listopadu 12, CZ-771 46 Olomouc, Czech Republic b Univ Hosp Olomouc, Dept. Forens Med & Med Law, Hnevotinska 3, Olomouc 77509, Czech Republic c Department of Physics and Materials Engineering, Faculty of Technology, Tomas Bata University in Zlin, nam. T.G. Masaryka 275, 76001 Zlin, Czech Republic d Department of Chemistry, University of Ioannina, Ioannina 451 10, Greece e Department of Chemistry, Faculty of Science, Masaryk University, Kamenice 5, 625 00 Brno, Czech Republic ⁎ Corresponding author. E-mail address: jhrbac@mail.muni.cz (J. Hrbac).
utb.fulltext.dates	Received 22 January 2018 Received in revised form 16 March 2018 Accepted 20 March 2018 Available online 21 March 2018
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utb.fulltext.sponsorship	Financial Support from Grant Agency of the Czech Republic, project No. 15-05198S and Palacky University student grant IGA_PrF_2018_027 is gratefully acknowledged. The authors wish to thank Katerina Krcova, BSc. for assistance with electrochemical measurements.
utb.wos.affiliation	[Rozsypal, Jan; Riman, Daniel; Opletal, Tomas; Jirovsky, David] Palacky Univ, Fac Sci, Dept Analyt Chem, 17 Listopadu 12, CZ-77146 Olomouc, Czech Republic; [Halouzka, Vladimir] Univ Hosp Olomouc, Dept Forens Med & Med Law, Hnevotinska 3, Olomouc 77509, Czech Republic; [Halouzka, Vladimir] Tomas Bata Univ Zlin, Dept Phys & Mat Engn, Fac Technol, Nam TG Masaryka 275, Min 76001, Czech Republic; [Prodromidis, Mamas] Univ Ioannina, Dept Chem, GR-45110 Ioannina, Greece; [Hrbac, Jan] Masaryk Univ, Dept Chem, Fac Sci, Kamenice 5, Brno 62500, Czech Republic
utb.scopus.affiliation	Department of Analytical Chemistry, Palacky University, Faculty of Science, 17. listopadu 12, Olomouc, Czech Republic; Univ Hosp Olomouc, Dept. Forens Med & Med Law, Hnevotinska 3, Olomouc, Czech Republic; Department of Physics and Materials Engineering, Faculty of Technology, Tomas Bata University in Zlin, nam. T.G. Masaryka 275, Zlin, Czech Republic; Department of Chemistry, University of Ioannina, Ioannina, Greece; Department of Chemistry, Faculty of Science, Masaryk University, Kamenice 5, Brno, Czech Republic
utb.fulltext.projects	15-05198S
utb.fulltext.projects	IGA_PrF_2018_027