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Reaction of some 2-quinolone derivatives with phosphoryl chloride: Synthesis of novel phosphoric acid esters of 4-hydroxy-2-quinolone

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dc.title Reaction of some 2-quinolone derivatives with phosphoryl chloride: Synthesis of novel phosphoric acid esters of 4-hydroxy-2-quinolone en
dc.contributor.author Rudolf, Ondřej
dc.contributor.author Mrkvička, Vladimír
dc.contributor.author Lyčka, Antonín
dc.contributor.author Rouchal, Michal
dc.contributor.author Klásek, Antonín
dc.relation.ispartof Journal of Heterocyclic Chemistry
dc.identifier.issn 0022-152X Scopus Sources, Sherpa/RoMEO, JCR
dc.date.issued 2013
utb.relation.volume 50
utb.relation.issue SUPPL.1
dc.citation.spage E100
dc.citation.epage E110
dc.type article
dc.language.iso en
dc.publisher Wiley-Blackwell Publishing, Inc. en
dc.identifier.doi 10.1002/jhet.1082
dc.relation.uri http://onlinelibrary.wiley.com/doi/10.1002/jhet.1082/full
dc.description.abstract 3-Chloroquinoline-2,4-diones do not react with phosphoryl chloride, however, 2,4-dichloroquinolines and/or 4-chloroquinolin-2-ones are formed in the presence of N,N-dimethylaniline. Along with these compounds, small quantities of novel dihydrogen phosphates of 4-hydroxyquinolin-2-ones were isolated. We outline a simple procedure that allows for the preparation of these compounds in moderate to good yields. All compounds were characterized by 1H and 13C NMR, IR, EI-MS, and ESI-MS spectroscopy, and in select cases by 31P NMR spectroscopy. © 2013 HeteroCorporation. en
utb.faculty Faculty of Technology
dc.identifier.uri http://hdl.handle.net/10563/1003220
utb.identifier.obdid 43870229
utb.identifier.scopus 2-s2.0-84876889121
utb.identifier.wok 000318428200015
utb.identifier.coden JHTCA
utb.source j-scopus
dc.date.accessioned 2013-05-22T11:52:54Z
dc.date.available 2013-05-22T11:52:54Z
dc.rights.access openAccess
utb.contributor.internalauthor Rudolf, Ondřej
utb.contributor.internalauthor Mrkvička, Vladimír
utb.contributor.internalauthor Rouchal, Michal
utb.contributor.internalauthor Klásek, Antonín
utb.fulltext.affiliation Ondřej Rudolf,a ; Vladimír Mrkvička,a ; Antonín Lyčka,b,c ; Michal Rouchal,a ; Antonín Klásek a* a Department of Chemistry, Faculty of Technology, Tomas Bata University, 762 72 Zlín, Czech Republic b Research Institute for Organic Syntheses (VUOS), Rybitví 296, 532 18 Pardubice 20, Czech Republic c Department of Analytical Chemistry, Faculty of Chemical Technology University of Pardubice, 53210 Pardubice, Czech Republic *E-mail: klasek@ft.utb.cz
utb.fulltext.dates Received June 20, 2011
utb.fulltext.sponsorship This study was supported by the Ministry of Education, Youth and Sports of the Czech Republic (Grant No. MSM 7088352101), the Czech Science Foundation (Grant No.203/07/0320), and the internal grant of TBU in Zlín (No. IGA/10/FT/10/D), funded from the resources of specific university research. The authors thank Mrs. H. Geržová (Faculty of Technology, Tomas Bata University in Zlín) for technical help.
utb.fulltext.faculty Faculty of Technology
utb.fulltext.ou Department of Chemistry
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