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Novel Tandem Hydration/Cyclodehydration of a-Thiocyanatoketones to 2-Oxo-3-thiazolines. Application to Thiazolo[5,4-c]quinoline-2,4(3aH,5H)-dione Synthesis.

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dc.title Novel Tandem Hydration/Cyclodehydration of a-Thiocyanatoketones to 2-Oxo-3-thiazolines. Application to Thiazolo[5,4-c]quinoline-2,4(3aH,5H)-dione Synthesis. en
dc.contributor.author Klásek, Antonín
dc.contributor.author Mrkvička, Vladimír
dc.contributor.author Pevec, Andrej
dc.contributor.author Košmrlj, Janez
dc.relation.ispartof Journal of Organic Chemistry
dc.identifier.issn 0022-3263 Scopus Sources, Sherpa/RoMEO, JCR
dc.date.issued 2004
utb.relation.volume 69
utb.relation.issue 17
dc.citation.spage 5646
dc.citation.epage 5661
dc.type article
dc.language.iso en
dc.publisher American Chemical Society (ACS) en
dc.identifier.doi 10.1021/jo0493370
dc.relation.uri http://pubs.acs.org/doi/full/10.1021/jo0493370
dc.subject thiokyanatoketony cs
dc.subject hydratace cs
dc.subject cyklizace cs
dc.subject syntéza cs
dc.subject thiocyanatoketones en
dc.subject hydration en
dc.subject cyclization en
dc.subject synthesis en
dc.description.abstract Novel tandem hydration of a-thiocyanatoketones to thiocarbamates followed by in situ cyclodehydration to fused 2-oxo-3-thiazolines is described. Concentrated sulfuric acid was found to be critical for the reaction as both corresponding thiocyanates and thiocarbamates rapidly hydrolyze in the presence of water. cs
dc.description.abstract Novel tandem hydration of a-thiocyanatoketones to thiocarbamates followed by in situ cyclodehydration to fused 2-oxo-3-thiazolines is described. Concentrated sulfuric acid was found to be critical for the reaction as both corresponding thiocyanates and thiocarbamates rapidly hydrolyze in the presence of water. en
utb.faculty Faculty of Technology
dc.identifier.uri http://hdl.handle.net/10563/1000360
utb.identifier.rivid RIV/70883521:28110/04:63502548
utb.identifier.obdid 12052358
utb.identifier.scopus 2-s2.0-4043148446
utb.identifier.wok 000223278200017
utb.source j-riv
utb.contributor.internalauthor Klásek, Antonín
utb.contributor.internalauthor Mrkvička, Vladimír
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