TBU Publications
Repository of TBU Publications

Synthesis of 3-Thiocyanato-1H,3H-quinoline-2,4-diones

DSpace Repository

Show simple item record

dc.title Synthesis of 3-Thiocyanato-1H,3H-quinoline-2,4-diones en
dc.contributor.author Klásek, Antonín
dc.contributor.author Polis, Jiří
dc.contributor.author Mrkvička, Vladimír
dc.contributor.author Košmrlj, Janez
dc.relation.ispartof Journal of Heterocyclic Chemistry
dc.identifier.issn 0022-152X Scopus Sources, Sherpa/RoMEO, JCR
dc.date.issued 2002
utb.relation.volume 39
utb.relation.issue 6
dc.citation.spage 1315
dc.citation.epage 1320
dc.type article
dc.language.iso en
dc.publisher Hetero Corporation en
dc.identifier.doi 10.1002/jhet.5570390632
dc.relation.uri http://onlinelibrary.wiley.com/doi/10.1002/jhet.5570390632/abstract
dc.subject thiokyanace cs
dc.subject dirhodan cs
dc.subject 3-thiokyanatochinolin-2,4-diony cs
dc.subject thiocyanation en
dc.subject thiocyanogen en
dc.subject 3-thiocyanatoquinoline-2,4-diones en
dc.description.abstract 4-Hydroxy-1H-quinolin-2-ones react with thiocyanogen in acetic acid to give corresponding 3-thiocyanato-1H,3H-quinoline- 2,4-diones in good yields. In some cases, 3-bromo-1H,3H-quinoline-2,4-diones were isolated as minor reaction products. en
utb.faculty Faculty of Technology
dc.identifier.uri http://hdl.handle.net/10563/1000103
utb.identifier.rivid RIV/70883521:28110/02:63500555
utb.identifier.obdid 11052416
utb.identifier.scopus 2-s2.0-0036875232
utb.identifier.wok 000180476400032
utb.source j-riv
utb.contributor.internalauthor Klásek, Antonín
utb.contributor.internalauthor Polis, Jiří
utb.contributor.internalauthor Mrkvička, Vladimír
utb.fulltext.affiliation Antonín Klásek*, Jirí Polis, and Vladimír Mrkvička Department of Chemistry and Environmental Technology, Faculty of Technology, Tomas Bata University, 762 72 Zlín, Czech Republic Janez Košmrlj Faculty of Chemistry and Chemical Technology, University of Ljubljana, SI-1000 Ljubljana, Slovenia
utb.fulltext.dates Received June 10, 2002
utb.fulltext.references [1] S. Kafka, M. Kovář, A. Klásek, and T. Kappe, J. Heterocyclic Chem., 33, 1977 (1996). [2] A. Klásek and S. Kafka, J. Heterocyclic Chem., 35, 307 (1998). [3] R. D. Northcross and I. Paterson, Chem. Rev., 95, 2041 (1995); D. J. Faulkner, Nat. Prod. Rep., 12, 223 (1995). [4] B. Schnell and T. Kappe, Monatsh. Chem., 130, 1147 (1999); B. Schnell and T. Kappe, J. Heterocyclic Chem., 3 7, 911 (2000). [5] G. H. Hakimelahi and G. Just, Tetrahedron Letters, 21, 2119 (1980). [6] M. Mataugi, K. Murata, K. Gotanda, H. Nambu, G. Anilkumar, K. Matsumoto, and Y. Kita, J. Org. Chem., 66, 2434 (2001) and rerefences therein. [7] O. Prakash, H. Kaur, H. Batra, N. Rani, S. P. Singh, and R. M. Moriarty, J. Org. Chem., 66, 2019 (2001). [8] W. Stadlbauer, R. Laschober, H. Lutschounig, G. Schindler, and T. Kappe, Monatsh. Chem., 123, 617 (1992). [9] A. Klásek, K. Kořistek, J. Polis, and J. Košmrlj, Heterocycles, 48, 2309 (1998). [10a] A. Klásek, K. Kořistek, J. Polis, and J. Košmrlj, Tetrahedron , 56, 1551 (2000); [b] S. Kafka, A. Klásek, and J. Košmrlj, J. Org. Chem, 66, 6394 (2001). [11] W. Stadlbauer, O. Schmut, and T. Kappe, Monatsh. Chem., 111, 1005 (1980). [12] J. W. Huffman, J. Org. Chem, 26, 1470 (1961). [13] F. D. Toste, V. De Stefano, and I. W. J. Still, Synth. Commun., 25, 1277 (1995). [14] Y. Kita, T. Takeda, S. Mihara, B.A. Whelan, and H. Tohma, J. Org. Chem., 60, 7144 (1995). [15] Y. Kita, T. Takeda, T. Okumo, M. Egi, K. Iio, K. Kanaguchi, and S. Akai, Chem. Pharm. Bull, 45, 1887 (1997). [16] O. Prakash, N. Rani, V. Sharma, and R. M. Moriarty, Synlett, 1255 (1997). [17] H. Iranpoor, H. Firouzebadi, and H. R. Shatterian, J . Chem. Res., 676 (1999). [18] Y. S. Park and K. Kim, Tetrahedron Letters, 4 0, 6439 (1999). [19] A. Khazaei, A. Alizadeh, and R. G. Vaghei, Molecules, 6, 253 (2001). [20] Dainippon Pharm. Co., Ltd., Japan Patent 6903356 (1966); Chem. Abstr. 70, 87600n (1969).
utb.fulltext.sponsorship The Ministry of Education, Youth and Sports of the Czech Republic and the Ministry of Education, Science and Sport, Republic of Slovenia (Grant No. P0-0503-0103) supported this study. The authors thank to Mrs. H. Geržová for technical help.
Find Full text

Files in this item

Show simple item record