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Impact of grain size and structural changes on magnetic, dielectric, electrical, impedance and modulus spectroscopic characteristics of CoFe2O4nanoparticles synthesized by honey mediated sol-gel combustion method

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dc.title Impact of grain size and structural changes on magnetic, dielectric, electrical, impedance and modulus spectroscopic characteristics of CoFe2O4nanoparticles synthesized by honey mediated sol-gel combustion method en
dc.contributor.author Yadav, Raghvendra Singh
dc.contributor.author Kuřitka, Ivo
dc.contributor.author Vilčáková, Jarmila
dc.contributor.author Havlica, Jaromír
dc.contributor.author Másilko, Jiří
dc.contributor.author Kalina, Lukáš
dc.contributor.author Tkacz, Jakub
dc.contributor.author Švec, Jiří
dc.contributor.author Enev, Vojtěch
dc.contributor.author Hajdúchová, Miroslava
dc.relation.ispartof Advances in Natural Sciences: Nanoscience and Nanotechnology
dc.identifier.issn 2043-6262 OCLC, Ulrich, Sherpa/RoMEO, JCR
dc.date.issued 2017
utb.relation.volume 8
utb.relation.issue 4
dc.type article
dc.language.iso en
dc.publisher Institute of Physics Publishing
dc.identifier.doi 10.1088/2043-6254/aa853a
dc.relation.uri http://iopscience.iop.org/article/10.1088/2043-6254/aa853a/meta
dc.subject autoclaving techniqueconventional heating en
dc.subject gold nanoparticles-hydrothermal en
dc.subject gold nanoparticles-hydrothermal autoclaving technique-conventional heating technique-catalytic activity en
dc.subject technique-catalytic activity en
dc.description.abstract In this work CoFe2O4spinel ferrite nanoparticles were synthesized by honey mediated sol-gel combustion method and further annealed at higher temperature 500 °C, 700 °C, 900 °C and 1100 °C. The synthesized spinel ferrite nanoparticles is investigated by x-ray diffraction, Raman spectroscopy, Fourier transform infrared (FTIR) spectroscopy, thermogravimetric analysis/differential scanning calorimetry (TGA/DSC), field emission scanning electron microscopy, x-ray photoelectron spectroscopy and vibrating sample magnetometer. The x-ray diffraction study reveals face-centered cubic spinel cobalt ferrite crystal phase formation. The crystallite size and lattice parameter are increased with annealing temperature. Raman and Fourier transform infrared spectra also confirm spinel ferrite crystal structure of synthesized nanoparticles. The existence of cation at octahedral and tetrahedral site in cobalt ferrite nanoparticles is confirmed by x-ray photoelectron spectroscopy. Magnetic measurement shows increased saturation magnetization 74.4 emu g-1at higher annealing temperature 1100 °C, high coercivity 1347.3 Oe at lower annealing temperature 500 °C, and high remanent magnetization 32.3 emu g-1at 900 °C annealing temperature. The magnetic properties of synthesized ferrite nanoparticles can be tuned by adjusting sizes through annealing temperature. Furthermore, the dielectric constant and ac conductivity shows variation with frequency (1-107Hz), grain size and cation redistribution. The modulus spectroscopy study reveals the role of bulk grain and grain boundary towards the resistance and capacitance. The cole-cole plots in modulus formalism also well support the electrical response of nanoparticles originated from both grain and grain boundaries. The dielectric, electrical, magnetic, impedance and modulus spectroscopic characteristics of synthesized CoFe2O4spinel ferrite nanoparticles demonstrate the applicability of these nanoparticles for magnetic recording, memory devices and for microwave applications. © 2017 Vietnam Academy of Science & Technology. en
utb.faculty University Institute
dc.identifier.uri http://hdl.handle.net/10563/1007682
utb.identifier.obdid 43877130
utb.identifier.scopus 2-s2.0-85039073109
utb.source j-scopus
dc.date.accessioned 2018-01-15T16:31:39Z
dc.date.available 2018-01-15T16:31:39Z
dc.description.sponsorship LO1504, NPU, Northwestern Polytechnical University
dc.rights Attribution 3.0 International
dc.rights.uri http://creativecommons.org/licenses/by/3.0/
dc.rights.access openAccess
utb.ou Centre of Polymer Systems
utb.contributor.internalauthor Yadav, Raghvendra Singh
utb.contributor.internalauthor Kuřitka, Ivo
utb.contributor.internalauthor Vilčáková, Jarmila
utb.fulltext.affiliation Raghvendra Singh Yadav1, Ivo Kuřitka1, Jarmila Vilcakova1, Jaromir Havlica2, Jiri Masilko2, Lukas Kalina2, Jakub Tkacz2, Jiří Švec2, Vojtěch Enev2 and Miroslava Hajdúchová2 1 Centre of Polymer Systems, University Institute, Tomas Bata University in Zlín, Trida Tomase Bati 5678, 760 01 Zlín, Czechia 2 Materials Research Centre, Brno University of Technology, Purkyňova 464/118, 61200 Brno, Czechia E-mail: yadav@cps.utb.cz
utb.fulltext.dates Received 9 February 2017 Accepted for publication 26 July 2017 Published 29 August 2017
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utb.fulltext.sponsorship This work was supported by the Ministry of Education, Youth and Sports of the Czech Republic—Program NPU I (LO1504).
utb.scopus.affiliation Centre of Polymer Systems, University Institute, Tomas Bata University in Zlín, Trida Tomase Bati 5678, Zlín, Czech Republic; Materials Research Centre, Brno University of Technology, Purkyňova 464/118, Czechia, Brno, Czech Republic
utb.fulltext.projects LO1504
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