Microwave-assisted hydrothermal synthesis of Ag/ZnO sub-microparticles

Münster, Lukáš; Bažant, Pavel; Machovský, Michal; Kuřitka, Ivo

dc.title	Microwave-assisted hydrothermal synthesis of Ag/ZnO sub-microparticles	en
dc.contributor.author	Münster, Lukáš
dc.contributor.author	Bažant, Pavel
dc.contributor.author	Machovský, Michal
dc.contributor.author	Kuřitka, Ivo
dc.relation.ispartof	Materiali in Tehnologije
dc.identifier.issn	1580-2949 Scopus Sources, Sherpa/RoMEO, JCR
dc.date.issued	2015
utb.relation.volume	49
utb.relation.issue	2
dc.citation.spage	281
dc.citation.epage	284
dc.type	article
dc.language.iso	en
dc.publisher	Institut za Kovinske Materiale in Tehnologije Ljubljana - Institute of Metals Technology
dc.identifier.doi	10.17222/mit.2013.223
dc.relation.uri	http://mit.imt.si/Revija/mit152.html
dc.subject	zinc oxide	en
dc.subject	silver	en
dc.subject	nanoparticle	en
dc.subject	hydrothermal	en
dc.subject	microwave synthesis	en
dc.description.abstract	A fast and environmentally friendly, microwave-assisted, hydrothermal synthesis was utilized for the preparation of a Ag/ZnO hybrid system by using zinc acetate dihydrate and silver nitrate as the sources of ZU(2+) and Ag+, and hexamethylentetramine as the reducing and precipitating agent. The influence of the concentration was investigated by X-ray diffraction analysis, scanning electron microscopy and energy-dispersive analysis. It was found that the concentration has a strong effect on the morphology and proportion between the Ag and ZnO components of the prepared particulate materials. With a decreasing concentration, the morphology of the ZnO changed from twinned or single frustums to rod-like microparticles, whereas the silver morphology changed from large polygon-shaped microparticles to very small, spherical nanoparticles.	en
utb.faculty	University Institute
utb.faculty	Faculty of Technology
dc.identifier.uri	http://hdl.handle.net/10563/1004603
utb.identifier.rivid	RIV/70883521:28610/15:43873031!RIV16-MSM-28610___
utb.identifier.obdid	43873451
utb.identifier.scopus	2-s2.0-84929754934
utb.identifier.wok	000353936700018
utb.source	j-wok
dc.date.accessioned	2015-06-02T08:13:06Z
dc.date.available	2015-06-02T08:13:06Z
dc.description.sponsorship	internal grant of TBU in Zlin [IGA/FT/2013/014]; European Regional Development Fund (ERDF); national budget of the Czech Republic, within the Centre of Polymer Systems project [CZ.1.05/2.1.00/03.0111]; European Social Fund (ESF); national budget of the Czech Republic, within the "Advanced Theoretical and Experimental Studies of Polymer Systems" project [CZ.1.07/2.3.00/20.0104]
dc.rights.uri	http://mit.imt.si/
dc.rights.access	openAccess
utb.ou	Centre of Polymer Systems
utb.contributor.internalauthor	Münster, Lukáš
utb.contributor.internalauthor	Bažant, Pavel
utb.contributor.internalauthor	Machovský, Michal
utb.contributor.internalauthor	Kuřitka, Ivo
utb.fulltext.affiliation	Lukáš Münster1,2, Pavel Bažant1,2, Michal Machovský2, Ivo Kuřitka1,2 1 Polymer Centre, Faculty of Technology, Tomas Bata University in Zlin, Nam. T. G. Masaryka 275, 762 72 Zlin, Czech Republic 2 Centre of Polymer Systems, University Institute, Tomas Bata University in Zlin, Nad Ovcirnou 3685, 760 01 Zlin, Czech Republic l_munster@ft.utb.cz
utb.fulltext.dates	Prejem rokopisa – received: 2013-10-02; sprejem za objavo – accepted for publication: 2014-04-03
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utb.fulltext.sponsorship	The authors wish to thank the internal grant of TBU in Zlin No. IGA/FT/2013/014 funded from the resources of specific university research for financial support. This article was written with the support of the Operational Program "Research and Development for Innovations" co-funded by the European Regional Development Fund (ERDF) and the national budget of the Czech Republic, within the Centre of Polymer Systems project (reg. number: CZ.1.05/2.1.00/03.0111). This article was written with the support of the Operational Program "Education for Competitiveness" co-funded by the European Social Fund (ESF) and the national budget of the Czech Republic, within the "Advanced Theoretical and Experimental Studies of Polymer Systems" project (reg. number: CZ.1.07/2.3.00/20.0104).