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Microwave-assisted hydrothermal synthesis of Ag/ZnO sub-microparticles

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dc.title Microwave-assisted hydrothermal synthesis of Ag/ZnO sub-microparticles en
dc.contributor.author Münster, Lukáš
dc.contributor.author Bažant, Pavel
dc.contributor.author Machovský, Michal
dc.contributor.author Kuřitka, Ivo
dc.relation.ispartof Materiali in Tehnologije
dc.identifier.issn 1580-2949 Scopus Sources, Sherpa/RoMEO, JCR
dc.date.issued 2015
utb.relation.volume 49
utb.relation.issue 2
dc.citation.spage 281
dc.citation.epage 284
dc.type article
dc.language.iso en
dc.publisher Institut za Kovinske Materiale in Tehnologije Ljubljana - Institute of Metals Technology
dc.identifier.doi 10.17222/mit.2013.223
dc.relation.uri http://mit.imt.si/Revija/mit152.html
dc.subject zinc oxide en
dc.subject silver en
dc.subject nanoparticle en
dc.subject hydrothermal en
dc.subject microwave synthesis en
dc.description.abstract A fast and environmentally friendly, microwave-assisted, hydrothermal synthesis was utilized for the preparation of a Ag/ZnO hybrid system by using zinc acetate dihydrate and silver nitrate as the sources of ZU(2+) and Ag+, and hexamethylentetramine as the reducing and precipitating agent. The influence of the concentration was investigated by X-ray diffraction analysis, scanning electron microscopy and energy-dispersive analysis. It was found that the concentration has a strong effect on the morphology and proportion between the Ag and ZnO components of the prepared particulate materials. With a decreasing concentration, the morphology of the ZnO changed from twinned or single frustums to rod-like microparticles, whereas the silver morphology changed from large polygon-shaped microparticles to very small, spherical nanoparticles. en
utb.faculty University Institute
utb.faculty Faculty of Technology
dc.identifier.uri http://hdl.handle.net/10563/1004603
utb.identifier.rivid RIV/70883521:28610/15:43873031!RIV16-MSM-28610___
utb.identifier.obdid 43873451
utb.identifier.scopus 2-s2.0-84929754934
utb.identifier.wok 000353936700018
utb.source j-wok
dc.date.accessioned 2015-06-02T08:13:06Z
dc.date.available 2015-06-02T08:13:06Z
dc.description.sponsorship internal grant of TBU in Zlin [IGA/FT/2013/014]; European Regional Development Fund (ERDF); national budget of the Czech Republic, within the Centre of Polymer Systems project [CZ.1.05/2.1.00/03.0111]; European Social Fund (ESF); national budget of the Czech Republic, within the "Advanced Theoretical and Experimental Studies of Polymer Systems" project [CZ.1.07/2.3.00/20.0104]
dc.rights.uri http://mit.imt.si/
dc.rights.access openAccess
utb.ou Centre of Polymer Systems
utb.contributor.internalauthor Münster, Lukáš
utb.contributor.internalauthor Bažant, Pavel
utb.contributor.internalauthor Machovský, Michal
utb.contributor.internalauthor Kuřitka, Ivo
utb.fulltext.affiliation Lukáš Münster1,2, Pavel Bažant1,2, Michal Machovský2, Ivo Kuřitka1,2 1 Polymer Centre, Faculty of Technology, Tomas Bata University in Zlin, Nam. T. G. Masaryka 275, 762 72 Zlin, Czech Republic 2 Centre of Polymer Systems, University Institute, Tomas Bata University in Zlin, Nad Ovcirnou 3685, 760 01 Zlin, Czech Republic l_munster@ft.utb.cz
utb.fulltext.dates Prejem rokopisa – received: 2013-10-02; sprejem za objavo – accepted for publication: 2014-04-03
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utb.fulltext.sponsorship The authors wish to thank the internal grant of TBU in Zlin No. IGA/FT/2013/014 funded from the resources of specific university research for financial support. This article was written with the support of the Operational Program "Research and Development for Innovations" co-funded by the European Regional Development Fund (ERDF) and the national budget of the Czech Republic, within the Centre of Polymer Systems project (reg. number: CZ.1.05/2.1.00/03.0111). This article was written with the support of the Operational Program "Education for Competitiveness" co-funded by the European Social Fund (ESF) and the national budget of the Czech Republic, within the "Advanced Theoretical and Experimental Studies of Polymer Systems" project (reg. number: CZ.1.07/2.3.00/20.0104).
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