Microwave-assisted hydrothermal synthesis of Ag/ZnO sub-microparticles

Münster, Lukáš; Bažant, Pavel; Machovský, Michal; Kuřitka, Ivo

dc.title	Microwave-assisted hydrothermal synthesis of Ag/ZnO sub-microparticles	en
dc.contributor.author	Münster, Lukáš
dc.contributor.author	Bažant, Pavel
dc.contributor.author	Machovský, Michal
dc.contributor.author	Kuřitka, Ivo
dc.relation.ispartof	Materiali in Tehnologije
dc.identifier.issn	1580-2949 Scopus Sources, Sherpa/RoMEO, JCR
dc.date.issued	2015
utb.relation.volume	49
utb.relation.issue	2
dc.citation.spage	281
dc.citation.epage	284
dc.type	article
dc.language.iso	en
dc.publisher	Institut za Kovinske Materiale in Tehnologije Ljubljana - Institute of Metals Technology
dc.identifier.doi	10.17222/mit.2013.223
dc.relation.uri	http://mit.imt.si/Revija/mit152.html
dc.subject	zinc oxide	en
dc.subject	silver	en
dc.subject	nanoparticle	en
dc.subject	hydrothermal	en
dc.subject	microwave synthesis	en
dc.description.abstract	A fast and environmentally friendly, microwave-assisted, hydrothermal synthesis was utilized for the preparation of a Ag/ZnO hybrid system by using zinc acetate dihydrate and silver nitrate as the sources of ZU(2+) and Ag+, and hexamethylentetramine as the reducing and precipitating agent. The influence of the concentration was investigated by X-ray diffraction analysis, scanning electron microscopy and energy-dispersive analysis. It was found that the concentration has a strong effect on the morphology and proportion between the Ag and ZnO components of the prepared particulate materials. With a decreasing concentration, the morphology of the ZnO changed from twinned or single frustums to rod-like microparticles, whereas the silver morphology changed from large polygon-shaped microparticles to very small, spherical nanoparticles.	en
utb.faculty	University Institute
utb.faculty	Faculty of Technology
dc.identifier.uri	http://hdl.handle.net/10563/1004603
utb.identifier.rivid	RIV/70883521:28610/15:43873031!RIV16-MSM-28610___
utb.identifier.obdid	43873451
utb.identifier.scopus	2-s2.0-84929754934
utb.identifier.wok	000353936700018
utb.source	j-wok
dc.date.accessioned	2015-06-02T08:13:06Z
dc.date.available	2015-06-02T08:13:06Z
dc.description.sponsorship	internal grant of TBU in Zlin [IGA/FT/2013/014]; European Regional Development Fund (ERDF); national budget of the Czech Republic, within the Centre of Polymer Systems project [CZ.1.05/2.1.00/03.0111]; European Social Fund (ESF); national budget of the Czech Republic, within the "Advanced Theoretical and Experimental Studies of Polymer Systems" project [CZ.1.07/2.3.00/20.0104]
dc.rights.uri	http://mit.imt.si/
dc.rights.access	openAccess
utb.ou	Centre of Polymer Systems
utb.contributor.internalauthor	Münster, Lukáš
utb.contributor.internalauthor	Bažant, Pavel
utb.contributor.internalauthor	Machovský, Michal
utb.contributor.internalauthor	Kuřitka, Ivo
utb.fulltext.affiliation	Lukáš Münster1,2, Pavel Bažant1,2, Michal Machovský2, Ivo Kuřitka1,2 1 Polymer Centre, Faculty of Technology, Tomas Bata University in Zlin, Nam. T. G. Masaryka 275, 762 72 Zlin, Czech Republic 2 Centre of Polymer Systems, University Institute, Tomas Bata University in Zlin, Nad Ovcirnou 3685, 760 01 Zlin, Czech Republic l_munster@ft.utb.cz
utb.fulltext.dates	Prejem rokopisa – received: 2013-10-02; sprejem za objavo – accepted for publication: 2014-04-03
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utb.fulltext.sponsorship	The authors wish to thank the internal grant of TBU in Zlin No. IGA/FT/2013/014 funded from the resources of specific university research for financial support. This article was written with the support of the Operational Program "Research and Development for Innovations" co-funded by the European Regional Development Fund (ERDF) and the national budget of the Czech Republic, within the Centre of Polymer Systems project (reg. number: CZ.1.05/2.1.00/03.0111). This article was written with the support of the Operational Program "Education for Competitiveness" co-funded by the European Social Fund (ESF) and the national budget of the Czech Republic, within the "Advanced Theoretical and Experimental Studies of Polymer Systems" project (reg. number: CZ.1.07/2.3.00/20.0104).
utb.scopus.affiliation	Münster L., Polymer Centre, Faculty of Technology, Tomas Bata University in Zlin, Nam. T. G. Masaryka 275, Zlin, 762 72, Czech Republic, Centre of Polymer Systems, University Institute, Tomas Bata University in Zlin, Nad Ovcirnou 3685, Zlin, 760 01, Czech Republic; Bažant P., Polymer Centre, Faculty of Technology, Tomas Bata University in Zlin, Nam. T. G. Masaryka 275, Zlin, 762 72, Czech Republic, Centre of Polymer Systems, University Institute, Tomas Bata University in Zlin, Nad Ovcirnou 3685, Zlin, 760 01, Czech Republic; Machovský M., Centre of Polymer Systems, University Institute, Tomas Bata University in Zlin, Nad Ovcirnou 3685, Zlin, 760 01, Czech Republic; Kuřitka I., Polymer Centre, Faculty of Technology, Tomas Bata University in Zlin, Nam. T. G. Masaryka 275, Zlin, 762 72, Czech Republic, Centre of Polymer Systems, University Institute, Tomas Bata University in Zlin, Nad Ovcirnou 3685, Zlin, 760 01, Czech Republic