Microwave assisted hydrothermal synthesis of Ag-ZnO nano-micro structures: Comparison of closed and open vessel reactor influence on nitrate solution preparation route

Bažant, Pavel; Kožáková, Zuzana; Kuřitka, Ivo; Machovský, Michal

dc.title	Microwave assisted hydrothermal synthesis of Ag-ZnO nano-micro structures: Comparison of closed and open vessel reactor influence on nitrate solution preparation route	en
dc.contributor.author	Bažant, Pavel
dc.contributor.author	Kožáková, Zuzana
dc.contributor.author	Kuřitka, Ivo
dc.contributor.author	Machovský, Michal
dc.relation.ispartof	NANOCON 2012
dc.identifier.isbn	978-80-87294-32-1
dc.identifier.isbn	978-80-87294-35-2
dc.date.issued	2012
dc.citation.spage	209
dc.citation.epage	214
dc.event.title	4th International Conference on NANOCON
dc.event.location	Brno
utb.event.state-en	Czech Republic
utb.event.state-cs	Česká republika
dc.event.sdate	2012-10-23
dc.event.edate	2012-10-25
dc.type	conferenceObject
dc.language.iso	en
dc.publisher	TANGER Ltd.
dc.relation.uri	http://www.nanocon.eu/files/proceedings/04/reports/727.pdf
dc.subject	microwave synthesis	en
dc.subject	Ag-ZnO nanostructures	en
dc.subject	ZnO microstructures	en
dc.description.abstract	Various Ag-ZnO nanostructures were synthesized by open vessel microwave system MWG1K-10 with reflux system and by pressurized microwave system CEM MARS 5. The material was prepared by microwave synthesis using soluble silver and zinc salts as source materials and hexamethylenetetramine as precipitating agent for ZnO and reducing agent for Ag. Influence of Ag+ ions, reaction condition and pressure by the pressurized microwave system on formation of particle microstructure was investigated. Scanning electron microscopy (SEM), Energy dispersive X-ray analyse (EDX) and powder X-ray difractometry (XRD) was used in order to investigate the morphology, phase composition and crystalline structure.	en
utb.faculty	Faculty of Technology
utb.faculty	University Institute
dc.identifier.uri	http://hdl.handle.net/10563/1003743
utb.identifier.rivid	RIV/70883521:28110/12:43869315!RIV13-MSM-28110___
utb.identifier.rivid	RIV/70883521:28610/12:43869315!RIV13-MSM-28610___
utb.identifier.obdid	43869586
utb.identifier.scopus	2-s2.0-84923683389
utb.identifier.wok	000333697100038
utb.source	d-wok
dc.date.accessioned	2014-06-05T20:22:59Z
dc.date.available	2014-06-05T20:22:59Z
utb.ou	Centre of Polymer Systems
utb.contributor.internalauthor	Bažant, Pavel
utb.contributor.internalauthor	Kožáková, Zuzana
utb.contributor.internalauthor	Kuřitka, Ivo
utb.contributor.internalauthor	Machovský, Michal
utb.fulltext.affiliation	Pavel BAZANT a,b, Zuzana KOZAKOVA a,b , Ivo KURITKA a,b , Michal MACHOVSKY a,b a Centre of Polymer Systems, University Institute, Tomas Bata University in Zlin, Nad Ovcirnou 3685, 760 01 Zlin, Czech Republic. b Polymer Centre, Faculty of Technology, Tomas Bata University in Zlin, Nam. T. G. Masaryka 275, 762 72 Zlin, Czech Republic. Corresponding author. Tel. +420 576 038 049; fax: +420 576 031 444. E-mail address: bazant@uni.utb.cz (P. Bazant).
utb.fulltext.dates	-
utb.fulltext.sponsorship	This article was written with support of Operational Program Education for Competitiveness cofunded by the European Social Fund (ESF) and national budget of Czech Republic, within the framework of project Advanced Theoretical and Experimental Studies of Polymer Systems (reg. number: CZ.1.07/2.3.00/20.0104). This article was written with support of Operational Program Research and Development for Innovations co-funded by the European Regional Development Fund (ERDF) and national budget of Czech Republic, within the framework of project Centre of Polymer Systems (reg. number: CZ.1.05/2.1.00/03.0111). The authors wish to thank the internal grant of TBU in Zlín No. IGA/FT/2012/042 funded from the resources of specific university research for financial support.
utb.fulltext.faculty	Faculty of Technology
utb.fulltext.faculty	University Institute
utb.fulltext.ou	Centre of Polymer Systems
utb.fulltext.ou	Polymer Centre